HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 2-(3-aminophenoxy)acetate → HCID 178433202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 2-(3-aminophenoxy)acetate | HCID 10561049 | — |
| Reactant | HCID 178433209 | HCID 178433209 | — |
| Solvent | Dichloromethane ethylacetate | HCID 21226138 | — |
| Product | HCID 178433202 | HCID 178433202 | — |
Reaction Steps
2-Guanidino-4-methyl-thiazole-5-carboxylic acid is reacted with tert-butyl (3-amino-phenoxy)-acetate in the same manner as in Example 3. Chromatography on silica gel with methylene chloride-ethyl acetate and methylene chloride-alcohol gives 176 mg of tert-butyl {3-[(2-guanidino-4-methyl-thiazole-5-carbonyl)-amino]-phenoxy}-acetate, m.p. 204° C., MS: 406 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297266B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-c68db61d470048ba9a00c0facda94b3f |
| Source note | uspto-grants-2001_10 |