化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Carbonate → Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 4-Nitrodiphenylamine | HCID 13271 | — |
| 反応物 | Methyl bromoacetate | HCID 60984 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Methyl [(4-nitro-phenyl)-phenyl-amino]-acetate | HCID 54362794 | — |
反応手順
4-Nitro-diphenylamine (Aldrich) is reacted with methyl bromoacetate in the presence of potassium carbonate in DMF at 70° C. to give methyl [(4-nitro-phenyl)-phenyl-amino]-acetate (brown oil). MS: 287 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06297266B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-4befb3919eea43d0a93eef70b3a9de60 |
| 出典メモ | uspto-grants-2001_10 |