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HRID379001

反应详情

EQUATION

反应方程式

HRID 379001 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=[N+]([O-])c1ccc(Nc2ccccc2)cc1
HCID13271

4-Nitro-N-phenylaniline

C12H10N2O2

结构：COC(=O)CBr
HCID60984

Methyl bromoacetate

C3H5BrO2

PRODUCTS

生成物

1
结构：COC(=O)CN(c1ccccc1)c1ccc([N+](=O)[O-])cc1
HCID54362794

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

4-Nitro-diphenylamine (Aldrich) is reacted with methyl bromoacetate in the presence of potassium carbonate in DMF at 70° C. to give methyl [(4-nitro-phenyl)-phenyl-amino]-acetate (brown oil). MS: 287 (M+1).