HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21696955, compound → HCID 21696967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21696955 | HCID 21696955 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21696967 | HCID 21696967 | — |
Reaction Steps
(4-Bromo-3-fluoro-phenyl)-(4-chloro-phenyl)-methanol (2.26 g, 7.16 mmol) and MnO2 (6.22 g, 70.1 mmol) was stirred in CH2Cl2 (40 mL) for 40 hr. The solution was filtered through a celite pad and concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297239B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-aac76817a0784ea096d2850178380bf0 |
| Source note | uspto-grants-2001_10 |