HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → HCID 178475091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | N5-(iminomethoxymethyl)-L-ornithine dihydrochloride | HCID 86583873 | — |
| Reactant | HCID 178475093 | HCID 178475093 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178475091 | HCID 178475091 | — |
Reaction Steps
From 1.3 g (3.17 mmol) N2-(tert-butoxycarbonyl)-N6-(ethoxyiminomethyl)-L-lysine tert-butyl ester hydrohloride was prepared 0.82 g (89%) N6-(ethoxyiminomethy)-L-lysine dihydrochloride by the method described above for the preparaton of N5-(iminomethoxymethyl)-L-ornithine dihydrochloride. TLC (4% ammonium hydroxide: methanol) Rf=024. Mass spectrum (CI) 218 (MH+, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297276B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-7fb0e9ea1fb54711a3629686450e0162 |
| Source note | uspto-grants-2001_10 |