HRID379081

反应详情

EQUATION

反应方程式

HRID 379081 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

From 1.3 g (3.17 mmol) N2-(tert-butoxycarbonyl)-N6-(ethoxyiminomethyl)-L-lysine tert-butyl ester hydrohloride was prepared 0.82 g (89%) N6-(ethoxyiminomethy)-L-lysine dihydrochloride by the method described above for the preparaton of N5-(iminomethoxymethyl)-L-ornithine dihydrochloride. TLC (4% ammonium hydroxide: methanol) Rf=024. Mass spectrum (CI) 218 (MH+, 92%).