HRID37914

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID54361054

未命名化合物

PRODUCTS

生成物

HCID20253626

Propan-2-yl 3-bromo-2-oxopropanoate

C6H9BrO3

收率 124.2%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3776

Isopropanol

C3H8O

CONDITIONS

反应条件

温度: 20 °C

PROCEDURE

实验过程

To iso-propanol was added 3-bromopyruvic chloride (5 g) at −5° C. dropwise and the solution was stirred overnight at 20° C. Evaporation of solvent gave iso-propyl 3-bromopyruvate (3.5 g), which was used in the next step without further purification.

WORKUP

后处理

customEvaporation of solvent