Cyclohexane → HCID 54040296, compound

HRID 379325Notes

Reaction equation

HRID 379325 reaction equation
[OH:1]C(C(=O)C=CC)C.[CH3:9][C:10]([CH2:15][CH2:16][CH3:17])([CH2:13][OH:14])[CH2:11][OH:12].[CH2:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1>>[OH:1][CH2:18][CH2:19][C:20]1([CH:21]=[CH:22][CH3:23])[O:14][CH2:13][C:10]([CH3:9])([CH2:15][CH2:16][CH3:17])[CH2:11][O:12]1

Participants

4

Reactant 3

HCID 8078CyclohexaneHCID 662202-Methyl-2-propylpropane-1,3-diolHCID 57075846HCID 57075846, compound

Product 1

HCID 54040296HCID 54040296, compound

Procedure

2.9 g of 2-hydroxyhex-4-en-3-one 63 (25 mmoles) and 3.3 g of 2-methyl-2-propylpropane-1.3-diol 24 (25 mmoles) are acetalized in 50 ml of cyclohexane by AAV 1. After distillation through a spinning band column, a clear light yellow oil is obtained.

Workup

  1. distillationAfter distillation through a spinning band column
  2. customa clear light yellow oil is obtained

Sources & evidence

ORD record
ord-cc52845d08df41cc9b836726c9876e6e
Source dataset
uspto-grants-2001_10
Patent number
US06297390B1

Reaction notes

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