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HRID379325

反应详情

EQUATION

反应方程式

HRID 379325 的结构方程式

REACTANTS

反应物

3
结构：C1CCCCC1
HCID8078

Cyclohexane

C6H12

结构：CCCC(C)(CO)CO
HCID66220

2-Methyl-2-propyl-1,3-propanediol

C7H16O2

结构：CC=CC(=O)C(C)O
HCID57075846

未命名化合物

PRODUCTS

生成物

1
结构：CC=CC1(CCO)OCC(C)(CCC)CO1
HCID54040296

未命名化合物

PROCEDURE

实验过程

2.9 g of 2-hydroxyhex-4-en-3-one 63 (25 mmoles) and 3.3 g of 2-methyl-2-propylpropane-1.3-diol 24 (25 mmoles) are acetalized in 50 ml of cyclohexane by AAV 1. After distillation through a spinning band column, a clear light yellow oil is obtained.

WORKUP

后处理

  1. distillationAfter distillation through a spinning band column
  2. customa clear light yellow oil is obtained