HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexane → HCID 54040296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexane | HCID 8078 | — |
| Reactant | 2-Methyl-2-propylpropane-1,3-diol | HCID 66220 | — |
| Reactant | HCID 57075846 | HCID 57075846 | — |
| Product | HCID 54040296 | HCID 54040296 | — |
Reaction Steps
2.9 g of 2-hydroxyhex-4-en-3-one 63 (25 mmoles) and 3.3 g of 2-methyl-2-propylpropane-1.3-diol 24 (25 mmoles) are acetalized in 50 ml of cyclohexane by AAV 1. After distillation through a spinning band column, a clear light yellow oil is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06297390B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-cc52845d08df41cc9b836726c9876e6e |
| Source note | uspto-grants-2001_10 |