Hydrochloric Acid → HCID 9936973, compound

Participants

Reaction Conditions

Reaction Steps

To 125 mg 1-(3,5-bis-trifluoromethyl-phenyl)-cyclopropanecarboxylic acid [4-(2-chlorophenyl)-pyridin-3-yl]-methyl-amide were added 1.5 ml 3 N hydrochloric acid in methanol. After evaporating the solution 3 ml ether were added and the suspension was stirred for 1 h at 0° C. Filtration afforded 100 mg (75%) of the title compound as white crystals. Mp.: 194-196° C.

Provenance & Evidence