HRID379673

反应详情

EQUATION

反应方程式

HRID 379673 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2,4 g (0.01 mol) of 6-trifluoroacetylamino-quinoline are dissolved in 20 ml glacial acetic acid and hydrogenated for I hour with 0.6 g platinum oxide at 3 bar. Then the catalyst is suction filtered and the solution is concentrated by evaporation. The residue is washed with a little sodium hydrogen carbonate solution and dried.

WORKUP

后处理

  1. filtrationfiltered
  2. concentrationthe solution is concentrated by evaporation
  3. washThe residue is washed with a little sodium hydrogen carbonate solution
  4. customdried