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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 379682Generated: October 30, 2026

Hydrochloric Acid → HCID 18366841, compound

https://huagongshe.com/reaction/379682

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantChlorosulfonic acidHCID 24638—
ReactantHCID 18366931HCID 18366931—
ProductHCID 18366841HCID 18366841—

Reaction Conditions

Temperature60 °C

Reaction Steps

(0.04 mol) of 1-[3-(4-cyano-phenyl)-propionyl]-1,2,3,4-tetrahydro-quinoline are dissolved in 16 ml of chlorosulphonic acid at 0° C. The thickly liquid mass is heated to 60° C. and hydrochloric acid develops. Then the mixture is carefully added to ice and extracted with methylene chloride, dried and concentrated by rotary evaporation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06300342B1
Source datasetuspto-grants-2001_10
ORD IDord-5285b9ba5df04fb09050cbddc416de01
Source noteuspto-grants-2001_10