HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 17910543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 17910569 | HCID 17910569 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17910543 | HCID 17910543 | — |
Reaction Steps
370 mg of 1-[3-(4-amidino-phenyl)propionyl]-6-(N-ethoxycarbonylmethyl-phenylsulphonamido)-1,2,3,4-tetrahydro-quinoline are dissolved in 5 ml of ethanol and stirred overnight with 1.6 ml of 1N sodium hydroxide solution. Then the mixture is neutralised with hydrochloric acid, concentrated by evaporation and the residue is chromatographed with methanol over a silica gel column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300342B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-beeaafdc6ad54fd4b0dc957f60bce999 |
| Source note | uspto-grants-2001_10 |