HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18368279, compound → HCID 18368323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18368279 | HCID 18368279 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18368323 | HCID 18368323 | 99.5% |
Reaction Steps
N-isopropyl-2-(2-methoxy-4-nitrophenoxy)ethylamine (9.29 g) solution in methanol (100 ml) was added with 10% palladium carbon catalyst and subjected to hydrogenation reaction at ambient pressure. After completion of hydrogenation reaction, catalyst was removed by filtration. Filtrate was concentrated under vacuum to obtain 4-[2-(isopropylamino)ethoxy]-3-methoxyaniline (8.15 g) as yellowish oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300368B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-1f6b31c8883847aaa2bec2bf041ebf8a |
| Source note | uspto-grants-2001_10 |