HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53740103, compound → HCID 18368270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53740103 | HCID 53740103 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18368270 | HCID 18368270 | 99% |
Reaction Steps
N-isopropyl-[2-(2,6-dimethyl-4-nitrophenoxy)]ethylamine (5.5 g) solution in methanol (70 ml) was subjected to hydrogenation reaction with 10% palladium carbon catalyst at ambient pressure. After completion of hydrogenation reaction, catalyst was removed by filtration. Filtrate was concentrated to obtain 4-[2-(isopropylamino) ethoxy]3,5-dimethylaniline (4.80 g) as pale brownish oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300368B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-4f9d8cb2477e4a4d85cebc620356965e |
| Source note | uspto-grants-2001_10 |