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HRID379759

反应详情

EQUATION

反应方程式

HRID 379759 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)(C)C(=O)Cl
HCID123496

2-Acetoxyisobutyroyl chloride

C6H9ClO3

结构：Nc1c(C(=O)c2ccccc2)[nH]c2cc(Cl)ccc12
HCID18367972

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)OC(C)(C)C(=O)Nc1c(C(=O)c2ccccc2)[nH]c2cc(Cl)ccc12
HCID18367845

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 19 employing 3-amino-2-benzoyl-6-chloroindole (Example 1) and 2-acetoxyisobutyryl chloride. m.p.: 162-165° C. 1H-NMR (CDCl3) δ: 10.78 (1H, br s), 8.36 (1H, d, J=9.2 Hz), 8.28 (1H, br s), 7.85-7.76 (2H, m), 7.68-7.53 (3H, m), 7.26 (1H, d, J=1.8 Hz), 7.08 (1H, dd, J=1.8, 9.2 Hz), 2.21 (3H, s), 1.75 (6H, s)