HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 18368220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 18367800 | HCID 18367800 | — |
| Product | HCID 18368220 | HCID 18368220 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 19 employing 3-amino-6-chloro-2-trimethylacetylindole (Example 89) and acetyl chloride. m.p.: 190-193° C. 1H-NMR (CDCl3) δ: 10.46 (1H, br s), 8.40 (1H, br s), 8.22 (1H, d, J=9.2 Hz), 7.29 (1H, s), 7.05 (1H, d, J=9.2 Hz), 2.29 (3H, s), 1.42 (9H, s)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-94305ede676844d9be4b11361d0b877d |
| Source note | uspto-grants-2001_10 |