3-Amino-2-(3-chlorobenzoyl)-1-(ethoxycarbonyl)-5-nitroindole → 3-Amino-2-(3-chlorobenzoyl)-5-nitroindole

HRID 379786Notes

Reaction equation

HRID 379786 reaction equation
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[CH:9]=2)[N:4](C(OCC)=O)[C:3]=1[C:19](=[O:27])[C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([Cl:26])[CH:21]=1>C(OCC)(=O)C>[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[CH:9]=2)[NH:4][C:3]=1[C:19](=[O:27])[C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([Cl:26])[CH:21]=1

Participants

3

Reactant 1

HCID 183679173-Amino-2-(3-chlorobenzoyl)-1-(ethoxycarbonyl)-5-nitroindole

Product 1

HCID 183679793-Amino-2-(3-chlorobenzoyl)-5-nitroindole

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The title compound was prepared according to the procedure described in step 3 of Example 1 from 3-amino-2-(3-chlorobenzoyl)-1-(ethoxycarbonyl)-5-nitroindole (step 1). tlc: Rf=0.3 (33% ethyl acetate in hexanes)

Sources & evidence

ORD record
ord-280630c48e2e4a6dbac1741e48f4dc7a
Source dataset
uspto-grants-2001_10
Patent number
US06300363B1

Reaction notes

Loading…