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HRID379787

反应详情

EQUATION

反应方程式

HRID 379787 的结构方程式

REACTANTS

反应物

2
结构：CC(C)CC(=O)Cl
HCID66054

Butanoyl chloride, 3-methyl-

C5H9ClO

结构：Nc1c(C(=O)c2cccc(Cl)c2)[nH]c2ccc([N+](=O)[O-])cc12
HCID18367979

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CC(=O)Nc1c(C(=O)c2cccc(Cl)c2)[nH]c2ccc([N+](=O)[O-])cc12
HCID18367766

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in Example 19 employing 3-amino-2-(3-chlorobenzoyl)-5-nitroindole (step 2) and isovaleryl chloride. m.p.: 197-199° C. 1H-NMR (CDCl3) δ: 9.91 (1H, br s), 9.37 (1H, d, J=2.2 Hz), 8.73 (1H, br.s), 8.24 (1H, dd, J=2.2, 9.2 Hz), 7.51-7.80 (4H, m), 7.38 (1H, d, J=9.2 Hz),2.37 (2H, br.s), 2.24-2.29 (1H, m), 1.07 (3H, s), 1.05 (3H, s)