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HRID379788

反应详情

EQUATION

反应方程式

HRID 379788 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc(C(=O)CBr)c1
HCID10036129

2-Bromo-1-(3-methylphenyl)ethan-1-one

C9H9BrO

结构：CCOC(=O)Nc1ccc([N+](=O)[O-])cc1C#N
HCID18367946

Ethyl (2-cyano-4-nitrophenyl)carbamate

C10H9N3O4

PRODUCTS

生成物

1
结构：CCOC(=O)n1c(C(=O)c2cccc(C)c2)c(N)c2cc([N+](=O)[O-])ccc21
HCID18368201

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in step 2 of Example 1 from 2-(ethoxycarbonylarnino)-5-nitrobenzonitrile (Example 96, step 1) and 2-bromo-3′-methylacetophenone. tlc: Rf=0.6 (33% ethyl acetate in hexanes)