Phenacyl bromide → HCID 18367847, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 1 from 2-(ethoxycarbonylamino)-4-fluorobenzonitrile (step 1) and 2-bromoacetophenone. 1H-NMR (CDCl3) δ: 7.94 (1H, dd, J=2.7, 10.3 Hz), 7.76-7.72 (2H, m), 7.57 (1H, dd, J=5.5, 8.8 Hz), 7.51-7.39 (3H, m), 7.06 (1H, ddd, J=2.7, 8.8, 10.3 Hz), 5.87 (2H, br s), 3.74 (2H, q, J=7.3 Hz), 0.84 (3H, t, J=7.3 Hz)

Provenance & Evidence