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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 379810Generated: October 31, 2026

HCID 18367790, compound → HCID 18368037, compound

https://huagongshe.com/reaction/379810

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18367790HCID 18367790—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 18368037HCID 18368037—

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 2 (Method A) from 3-acetylamino-5-bromo-6-chloro-1-(ethoxycarbonyl)-2-(6-methylpyridine-2-carbonyl)indole (step 2). m.p.: 234-236° C. (dichloromethane/methanol) 1H-NMR (DMSO-d6) δ: 12.01 (1H, br s), 10.26 (1H, br s), 8.21 (1H, s), 7.98 (1H, t, J=7.7 Hz), 7.86 (1H, d, J=7.7 Hz), 7.85 (1H, s), 7.57 (1H, d, J=7.7 Hz), 2.66 (3H, s), 1.99 (3H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06300363B1
Source datasetuspto-grants-2001_10
ORD IDord-3181b67c5a0f42d1bf15c062eb87f522
Source noteuspto-grants-2001_10