HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18367790, compound → HCID 18368037, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18367790 | HCID 18367790 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 18368037 | HCID 18368037 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 2 (Method A) from 3-acetylamino-5-bromo-6-chloro-1-(ethoxycarbonyl)-2-(6-methylpyridine-2-carbonyl)indole (step 2). m.p.: 234-236° C. (dichloromethane/methanol) 1H-NMR (DMSO-d6) δ: 12.01 (1H, br s), 10.26 (1H, br s), 8.21 (1H, s), 7.98 (1H, t, J=7.7 Hz), 7.86 (1H, d, J=7.7 Hz), 7.85 (1H, s), 7.57 (1H, d, J=7.7 Hz), 2.66 (3H, s), 1.99 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-3181b67c5a0f42d1bf15c062eb87f522 |
| Source note | uspto-grants-2001_10 |