HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Trifluoropropionic acid → 2-Benzoyl-6-chloro-3-(3,3,3-trifluoropropionylamino)indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Trifluoropropionic acid | HCID 2777972 | — |
| Reactant | 3-Amino-2-benzoyl-6-chloroindole | HCID 18367972 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | 2-Benzoyl-6-chloro-3-(3,3,3-trifluoropropionylamino)indole | HCID 18367749 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 114 employing 3-amino-2-benzoyl-6-chloroindole (Example 1) and 3,3,3-trifluoropropionic acid. m.p.: 201-204° C. (ethyl acetate/hexane)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-dfc18caebbb94fb6925d35375db1dff5 |
| Source note | uspto-grants-2001_10 |