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HRID379835

反应详情

EQUATION

反应方程式

HRID 379835 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Cl
HCID6367

Acetyl chloride

C2H3ClO

结构：CCOC(=O)n1c(C(=O)c2cccc([N+](=O)[O-])c2)c(N)c2ccc(Cl)cc21
HCID18368058

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)n1c(C(=O)c2cccc([N+](=O)[O-])c2)c(NC(C)=O)c2ccc(Cl)cc21
HCID18367880

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in step 1 of Example 2 (Method A) from 3-amino-6-chloro-1-ethoxycarbonyl-2-(3-nitrobenzoyl)indole (step 1) and acetyl chloride. 1H-NMR (CDCl3) δ: 9.18 (1H, br s), 8.65-8.69 (1H, m), 8.38-8.42 (1H, m), 8.02-8.10 (1H, m), 7.98 (1H, s), 7.61-7.71 (2H, m), 7.18-7.25 (1H, m), 4.15 (2H, q, J=7.0 Hz), 2.24 (3H, s), 1.17 (3H, t, J=7.0 Hz)