HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18367942, compound → HCID 18368035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18367942 | HCID 18367942 | — |
| Solvent | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 18368035 | HCID 18368035 | 135.2% |
Reaction Steps
3-Acetylamino-2-(3-aminobenzoyl)-6-chloroindole (Example 135, 0.41 g, 1.3 mmol) was stirred in 10% HCl—MeOH (3.0 ml) for 10 min and then solvent removed by evaporation. The residual solid was recrystallized from ethanol/diethyl ether to afford 320 mg (70%) of the title compound as a yellow solid. m.p.:>300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-c5dc8ea541ae40ce8bc0782892008d5c |
| Source note | uspto-grants-2001_10 |