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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 379837Generated: October 30, 2026

HCID 18367942, compound → HCID 18368035, compound

https://huagongshe.com/reaction/379837

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 18367942HCID 18367942—
SolventHydrochloride methanolHCID 21893726—
ProductHCID 18368035HCID 18368035135.2%

Reaction Steps

3-Acetylamino-2-(3-aminobenzoyl)-6-chloroindole (Example 135, 0.41 g, 1.3 mmol) was stirred in 10% HCl—MeOH (3.0 ml) for 10 min and then solvent removed by evaporation. The residual solid was recrystallized from ethanol/diethyl ether to afford 320 mg (70%) of the title compound as a yellow solid. m.p.:>300° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06300363B1
Source datasetuspto-grants-2001_10
ORD IDord-c5dc8ea541ae40ce8bc0782892008d5c
Source noteuspto-grants-2001_10