HuagongsheHuagongshe Chemistry Print Report · For research reference only
[3,4-Bis(methoxymethoxy)]phenacyl chloride → HCID 18367762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [3,4-Bis(methoxymethoxy)]phenacyl chloride | HCID 18367805 | — |
| Reactant | 4-Chloro-2-[(ethoxycarbonyl)amino]benzonitrile | HCID 18367888 | — |
| Product | HCID 18367762 | HCID 18367762 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 1 from 4-chloro-2-(ethoxycarbonylamino)benzonitrile (Example 1, step 1) and [3,4-bis(methoxymethyloxy)]phenacyl chloride (step 1). 1H-NMR (CDCl3) δ: 8.25 (1H, d, J=1.8 Hz), 7.61 (1H, d, J=2.2 Hz), 7.52 (1H, d, J=8.0 Hz), 7.39 (1H, dd, J=8.4, 1.8 Hz), 7.29 (1H, dd, J=8.4, 1.8 Hz), 7.18 (1H, d, J=8.4 Hz), 5.72 (2H, br s), 5.29 (2H, s), 5.25 (2H, s), 3.86 (2H, q, J=7.3 Hz), 3.52 (6H, s), 0.91 (3H, t, J=7.3 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-dbbfe8ad8a194b5182654b6774b19ae1 |
| Source note | uspto-grants-2001_10 |