HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 3-(3-Acetylamino-6-chloroindole-2-carbonyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 3-(3-Amino-6-chloroindole-2-carbonyl)benzenesulfonamide | HCID 18367795 | — |
| Solvent | Toluene ethanol | HCID 21863594 | — |
| Product | 3-(3-Acetylamino-6-chloroindole-2-carbonyl)benzenesulfonamide | HCID 18367924 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 19 employing 3-(3-amino-6-chloroindole-2-carbonyl)benzenesulfonamide (Example 142) and acetyl chloride. m.p.: 250-251° C. (ethanol/toluene)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300363B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-b6809f1122ca4058852d5e01f0c15d37 |
| Source note | uspto-grants-2001_10 |