Ethyl Acetate → HCID 18367782, compound

HRID 379850Notes

Reaction equation

[C:1]([NH:4][C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[N:7](C(OCC)=O)[C:6]=1[C:20](=[O:28])[C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([Cl:27])[CH:22]=1)(=O)C.[C:29](OCC)(=[O:31])[CH3:30]>>[C:29]([N:4]([C:5]1[C:13]2[C:8](=[CH:9][C:10]([Cl:14])=[CH:11][CH:12]=2)[NH:7][C:6]=1[C:20](=[O:28])[C:21]1[CH:26]=[CH:25][CH:24]=[C:23]([Cl:27])[CH:22]=1)[CH3:1])(=[O:31])[CH3:30]

Participants

Reactant 2

HCID 8857Ethyl Acetate

HCID 18367754HCID 18367754, compound

Product 1

HCID 18367782HCID 18367782, compound

Procedure

The title compound was prepared from 3-acetylamino-6-chloro-2-(3-chlorobenzoyl)-1-(ethoxycarbonyl)indole (Example 31, step 1) according to the procedure described in Example 146. m.p.: 202-203° C. (ethyl acetate)

Sources & evidence

ORD record: ord-f144951810d5454bad30c6cc022999f2
Source dataset: uspto-grants-2001_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06300363B1

Reaction notes

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