Phenacyl bromide → HCID 18367760, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 1 from 2-(ethoxycarbonylamino)-4-nitrobenzonitrile (step 1) and 2-bromoacetophenone. 1H-NMR (CDCl3) δ: 9.13 (1H, d, J=1.8 Hz), 8.20 (1H, dd, J=1.8, 8.6 Hz), 7.74 (1H, d, J=8.6 Hz), 7.77-7.43 (5H, m), 5.67 (2H, br. s), 3.83 (2H, q, J=7.3 Hz), 0.89 (3H, t, J=7.3 Hz)

Provenance & Evidence