HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Bromobenzenesulphonyl chloride → HCID 18367592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18367592 | HCID 18367592 | 59.1% |
Reaction Steps
4-(2-Aminoethyl)morpholine (2.54 g) was added, dropwise to a stirred solution of 3-bromobenzenesulphonyl chloride (5.0 g) in ether (50 ml) at 5° C. The resulting suspension was stirred for 30 minutes and filtered to afford the sub-titled compound as a solid (4.45 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300352B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-c469a0099a874b08979df1542562e325 |
| Source note | uspto-grants-2001_10 |