HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pyrrolidineethanamine → HCID 18367625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pyrrolidineethanamine | HCID 1344 | — |
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18367625 | HCID 18367625 | 85.9% |
Reaction Steps
N-(2-Aminoethyl)pyrrolidine (1.61 g) was added dropwise to a solution of 3-bromobenzenesulfonyl chloride (3.61 g) in diethyl ether (100 ml) at room temperature. The resulting suspension was stirred for 30 minutes and filtered to afford the sub-title compound as a solid (4.48 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300352B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-dfe8c2c8deca40068cde13aa562b8032 |
| Source note | uspto-grants-2001_10 |