HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminothiophenol → HCID 20693371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminothiophenol | HCID 14510 | — |
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Product | HCID 20693371 | HCID 20693371 | — |
Reaction Steps
To a solution of 4-aminothiophenol (2.36 g) in tetrahydrofuran (THF; 20 ml), 2-propenoic acid t-butyl ester (3.51 ml) and 1.0M tetrabutylammonium fluoride in THF solution (340 μl) were added. The mixture solution was stirred for 30 minutes at room temperature to give the title compound. The compound was used for next reaction as such.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06300514B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-23f9daa70d264dc6b56fc72088adf0c6 |
| Source note | uspto-grants-2001_10 |