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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 380071Generated: November 1, 2026

4-Aminothiophenol → HCID 20693371, compound

https://huagongshe.com/reaction/380071

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-AminothiophenolHCID 14510—
Reactanttert-Butyl acrylateHCID 15458—
SolventTetrahydrofuranHCID 8028—
SolventTetrabutylammonium FluorideHCID 2724141—
ProductHCID 20693371HCID 20693371—

Reaction Steps

To a solution of 4-aminothiophenol (2.36 g) in tetrahydrofuran (THF; 20 ml), 2-propenoic acid t-butyl ester (3.51 ml) and 1.0M tetrabutylammonium fluoride in THF solution (340 μl) were added. The mixture solution was stirred for 30 minutes at room temperature to give the title compound. The compound was used for next reaction as such.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06300514B1
Source datasetuspto-grants-2001_10
ORD IDord-23f9daa70d264dc6b56fc72088adf0c6
Source noteuspto-grants-2001_10