Acryloyl chloride → 1-ADAMANTYL ACRYLATE

HRID 380273Notes

Reaction equation

HRID 380273 reaction equation
[C:1]12([OH:11])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:12](Cl)(=[O:15])[CH:13]=[CH2:14]>>[C:12]([O:11][C:1]12[CH2:8][CH:7]3[CH2:6][CH:5]([CH2:4][CH:3]([CH2:9]3)[CH2:2]1)[CH2:10]2)(=[O:15])[CH:13]=[CH2:14]

Participants

3

Reactant 2

HCID 13140Acryloyl chlorideHCID 641521-Adamantanol

Product 1

HCID 113901281-ADAMANTYL ACRYLATE

Procedure

1-Adamantanol and acrylic acid chloride were subjected to desalting reaction by using a basic catalyst to obtain adamantyl acrylate (Compound (III-h)).

Workup

  1. customreaction

Sources & evidence

ORD record
ord-e52753b52a3e431788da54f6d26410c4
Source dataset
uspto-grants-2001_10
Patent number
US06303266B1

Reaction notes

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