1-Bromo-3-chloropropane → HCID 18365020, compound

HRID 380343Notes

Reaction equation

HRID 380343 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[CH:18]=[CH:17][CH:16]=[CH:15][C:10]=2[C:11]([O:13][CH3:14])=[O:12])[CH:5]=[CH:6][CH:7]=1.Br[CH2:20][CH2:21][CH2:22][Cl:23]>>[Cl:23][CH2:22][CH2:21][CH2:20][O:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[CH:18]=[CH:17][CH:16]=[CH:15][C:10]=2[C:11]([O:13][CH3:14])=[O:12])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 18365045HCID 18365045, compound

Product 1

HCID 18365020HCID 18365020, compoundYield 85%

Procedure

It was prepared from methyl 2-(3-hydroxyphenylsulfanyl)-benzoate and 1-bromo-3-chloropropane as an oil in a yield of 85.0%. For C17H17ClO3S (336.8) calculated: 60.62% C, 5.09% H, 10.52% Cl, 9.52% S; found: 60.46% C, 5.09% H, 10.35% Cl, 9.42% S.

Sources & evidence

ORD record
ord-d3c7b54724cc4b7da84ddfb6bda2f673
Source dataset
uspto-grants-2001_10
Patent number
US06303612B1

Reaction notes

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