HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 15462363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 18349331 | HCID 18349331 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15462363 | HCID 15462363 | — |
Reaction Steps
3,5-diiodo-4-(4′-methoxyphenoxy)-N,N-dimethyl benzamide (Compound 9) was prepared way of 3,5-diiodo-4-(4′-methoxyphenoxy)benzoyl chloride (see, Example 1.5). The acid chloride was reacted with excess dimethylamine in tetrahydrofuran at ambient temperature (1 hour), filtered to remove dimethylamine-hydrochloride precipitate, the solvent evaporated and the product crystallized from absolute ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06303621B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-746e3b5665cd4e469755e969f6bb78cf |
| Source note | uspto-grants-2001_10 |