HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 18364916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 18364851 | HCID 18364851 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18364916 | HCID 18364916 | 99.8% |
Reaction Steps
A mixture of 0.35 g (1.18 mmol) of benzyl-3-methyl-2-phenylbenzoate and 0.25 g of 10% Pd/C in 8 mL of a 4.4% solution of HCO2H in methanol was heated at reflux for 2 h. The reaction mixture was filtered through a thin layer of celite and concentrated to give 0.25 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06303593B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-d9dd16dc50ba4dbf988cf6cfffa82204 |
| Source note | uspto-grants-2001_10 |