HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21779698, compound → HCID 18364729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21779698 | HCID 21779698 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18364729 | HCID 18364729 | 93.5% |
Reaction Steps
A mixture of 0.105 g (0.6 mmol) of methyl-2-vinyl-3-methylbenzoate and 0.05 g of Pd/C 10% in 15 mL of ethyl acetate was hydrogenated at 50 psi for 2 h. The reaction mixture was filtered through a thin pad of celite and the filtrate was concentrated to give 0.1 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06303593B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-ddf0572280da4aa1a8f53d5f77874bcf |
| Source note | uspto-grants-2001_10 |