Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | HCID 10396954 | HCID 10396954 | — |
| Product | HCID 18365250 | HCID 18365250 | 67.2% |
Reaction Steps
A mixture of 54.4 gm (0.374 mole) ethyl 3-(N-methyl-amino)butanoate and 100 gm (0.999 mole) ethyl acrylate was heated at 110° C. with stirring for 18 hours. The reaction mixture was cooled to room temperature and then distilled under reduced pressure to provide 61.7 gm (67.1%) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06303627B1 |
|---|
| Source dataset | uspto-grants-2001_10 |
|---|
| ORD ID | ord-2c904ad70673441f918ad7d0b557b80c |
|---|
| Source note | uspto-grants-2001_10 |
|---|
