Bromine → 6-Amino-7-bromobenzothiazole

HRID 380612Notes

Reaction equation

HRID 380612 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]2[N:6]=[CH:7][S:8][C:4]=2[CH:3]=1.[Br:11]Br.CCOC(C)=O.CCCCCC>CC(O)=O.CCOC(C)=O>[Br:11][C:3]1[C:4]2[S:8][CH:7]=[N:6][C:5]=2[CH:9]=[CH:10][C:2]=1[NH2:1]

Participants

6

Conditions

Temperature
25 °C

Procedure

To a solution of 6-aminobenzothiazole (16 g, 107 mmol) in 100 mL of AcOH was added Br2 (2.0 mL, 43 mmol) dropwise and the resulting reaction mixture was stirred for 1 h at 25° C. Reaction mixture was concentrated in vacuo, yielding a yellow solid which was dissolved in EtOAc and washed with aq. NaHCO3. Organic layer was dried over Na2SO4 and concentrated in vacuo, yielding an oil which was subjected to column chromatography (10-50% EtOAc/n-Hexane) to obtain 7.8 g (34 mmol, 80% ) of the desired product.

Workup

  1. customthe resulting reaction mixture
  2. customReaction mixture
  3. concentrationwas concentrated in vacuo
  4. customyielding a yellow solid which
  5. washwashed with aq. NaHCO3
  6. dry with materialOrganic layer was dried over Na2SO4
  7. concentrationconcentrated in vacuo
  8. customyielding an oil which

Sources & evidence

ORD record
ord-88a5e7a6c99342baa3100ee7104fb62c
Source dataset
uspto-grants-2001_10
Patent number
US06303643B1

Reaction notes

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