HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → (S)-3-(Benzyloxy)butanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Methyl (S)-3-benzyloxybutyrate | HCID 13967615 | — |
| Solvent | Water | HCID 962 | — |
| Product | (S)-3-(Benzyloxy)butanoic acid | HCID 11845529 | — |
Reaction Steps
To a solution of 8.73 g of potassium hydroxide in 140 mL of cold water was dissolved methyl (S)-3-benzyloxybutyrate (18) (24.21 g). The solution was stirred in an ice bath for one hour and at room temperature for one hour. Methanol was added to give a clear solution and the reaction was stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306828B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-0c7e407c581e4b0f91489d15f845d5b3 |
| Source note | uspto-grants-2001_10 |