HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 499733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 6-[1-[3-(Ethylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid methyl ester | HCID 70212253 | — |
| Product | HCID 499733 | HCID 499733 | 73% |
Reaction Steps
By the same procedure as described in the example 2, synthesis was carried out starting with 6-[1-[3-(ethylamino)-2-pyridyl]piperazin-4-yl-carbonyl]nicotinic acid methyl ester and using ethanolamine. And then, the product was recrystallized with ethanol and hexane to give a desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306860B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-f99fb160fcfb4eb28108b763c8461ed3 |
| Source note | uspto-grants-2001_10 |