HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 18362843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | HCID 18362798 | HCID 18362798 | — |
| Product | HCID 18362843 | HCID 18362843 | 72% |
Reaction Steps
By the same procedure as described in the step (2) of example 27, the synthesis was carried out starting with 5-[N-(2-methylpropyl)carbamoyl]-2-[1-(3-nitro-2-pyridyl)piperazin-4-yl-carbonyl]pyridine, so prepared by Step (1) and using isobutylamine. And then, the product was recrystallized with ethanol and ether to give a desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06306860B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-3175f943751f4db1b5ea6e858cbde720 |
| Source note | uspto-grants-2001_10 |