Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | HCID 11162497 | HCID 11162497 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 12994567 | HCID 12994567 | — |
Reaction Steps
2-(2′-Hydroxy-5′bromomethylphenyl)benzotriazole (3.03 g. 0.01 mole), diethanol amine (3.14 g. 0.03 mole) were dissolved in 100 ml. of acetone. The reaction mixture was refluxed with constant stirring at 75° C. for 6 h. The solvent was then removed by rotary evaporation. Crude product was purified using silica gel column chromatography Product was identified by 1H-NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06307055B1 |
|---|
| Source dataset | uspto-grants-2001_10 |
|---|
| ORD ID | ord-52553da4d89a4553936a6f652a607a00 |
|---|
| Source note | uspto-grants-2001_10 |
|---|
