HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 57483899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | N-Carbamylmaleimide | HCID 76868 | — |
| Product | HCID 57483899 | HCID 57483899 | 95% |
Reaction Steps
The addition of isopropanol to N-carbamylmaleimide under the conditions of Example C afforded a 95% yield of isopropyl maleurate. M.P.: 113°-14° C.; 1H NMR (CDCl3): δ10.6 (br s, 1H), 8.2 (br s, 1H), 6.3 (AB, 2H), 5.8 (br s, 1H), 5.2 (quintet, 1H), 1.3 (d, 6H); HPLC (20% CH3CN/H2O, C8): Rt=5.6 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06307058B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-1c1d7e0c86d4471886c48e64e66b1c8a |
| Source note | uspto-grants-2001_10 |