HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetic acid → 3-Ethyl-5-phenylpentanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | 1-Phenylpentan-3-one | HCID 88701 | — |
| Product | 3-Ethyl-5-phenylpentanenitrile | HCID 15907302 | — |
Reaction Steps
The reaction was repeated utilizing an equimolar quantity of dimethyl malonate in place of the cyanoacetic acid to yield methyl 4-methyl-5-phenylpentanoate. Repeating the cyanoacetic acid condensation/reduction reaction utilizing 5phenylpentan-3-one as the starting material afforded 3-ethyl-5-phenylpentanenitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310033B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-e54cbff81cdd4500bae92386282c837c |
| Source note | uspto-grants-2001_10 |