HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25204926, compound → HCID 178434539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25204926 | HCID 25204926 | — |
| Reactant | 1-(4-methoxybenzyl)-5-methyl-1H-pyrazole-4-carboximidamide | HCID 68611033 | — |
| Product | HCID 178434539 | HCID 178434539 | 37% |
Reaction Steps
According to Scheme 1 Step 4: The title compound was prepared according to Example 2 Step 4, from a mixture of 3-(1-(4-methoxybenzyl)-3-methyl-1H-pyrazol-4-yl)-N-(pyridin-2-yl)-1,2,4-thiadiazol-5-amine and of 1-(4-methoxybenzyl)-5-methyl-1H-pyrazole-4-carboximidamide (0.11 mmol, 43 mg). 11 mg (43 μmol, 37%) of 3-(3-methyl-1H-pyrazol-4-yl)-N-(pyridin-2-yl)-1,2,4-thiadiazol-5-amine were obtained as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524718B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-ccb75ca653f84c618805f7c91067e8e2 |
| Source note | uspto-grants-2013_09 |