HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 135708923, compound → HCID 135708849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 135708923 | HCID 135708923 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 135708849 | HCID 135708849 | 100% |
Reaction Steps
0.2 g of 10% palladium carbon was added to a solution of 0.9 g (1.90 mmol) of the resulting hypoxanthine compound in 50 ml of methanol and the mixture was stirred overnight in a hydrogen atmosphere. Palladium carbon was removed by filtration and the residue was concentrated under vacuum to obtain 0.64 g of 2-ethyl-7-(4-hydroxy-3,5-di-t-butylbenzyl)hypoxanthine (yield 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-d729c356fe454dfaa73f047bc3dd9c8a |
| Source note | uspto-grants-2001_10 |