HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzoyl chloride → HCID 18360369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | HCID 18360337 | HCID 18360337 | — |
| Product | HCID 18360369 | HCID 18360369 | 93% |
Reaction Steps
An amidation reaction and post-treatment were carried out following the conditions of Example 22, using 2.00 g (8.19 mmol) of 4-amino-1-(3-phenylpropyl)-5-imidazolecarboxamide prepared in the same manner as in Example 114 and 4-fluorobenzoyl chloride instead of benzoyl chloride to obtain 2.78 g of 4-(4-fluorobenzoylamino)-1-(3-phenylpropyl)-5-imidazolecarboxamide (yield 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-0a7e0dc571554e5fa12194785bec6cfb |
| Source note | uspto-grants-2001_10 |