HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolinic acid → HCID 18360294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolinic acid | HCID 1018 | — |
| Reactant | 1-benzyl-4-amino-1H-imidazole-5-carboxamide | HCID 14000620 | — |
| Product | HCID 18360294 | HCID 18360294 | 87% |
Reaction Steps
An amidation reaction and post-treatment were carried out following the conditions of Example 17, using 1.0 g (4.6 mmol) of 4-amino-1-benzyl-5-imidazolecarboxamide prepared in the same manner as in Reference Example 2 and picolinic acid instead of 3-pyridylacetic acid hydrochloride to obtain 1.29 g of 1-benzyl-4-(2-pyridylcarbonylamino)-5-imidazolecarboxamide (yield 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310070B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-acfe422203fb4a639f2cdfb76679e35a |
| Source note | uspto-grants-2001_10 |