HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → alpha-[2-(4-Methoxyphenylthio)5-furyl]-N-n-propylnitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | N-propylhydroxylamine | HCID 10148984 | — |
| Product | alpha-[2-(4-Methoxyphenylthio)5-furyl]-N-n-propylnitrone | HCID 73433665 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1 using 4-methoxybenzenethiol and N-n-propylhydroxylamine. The title compound was isolated in 76.6% yield as slightly yellowish crystals, m.p. 63.0° C. (Rf=0.17 on a silica gel plate using hexanes/EtOAc, 2:1, v:v, as the eluant).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310092B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-d93f40729421425189f637f8831b5ec3 |
| Source note | uspto-grants-2001_10 |